3CSL: Difference between revisions

64 bytes removed ,  19 December 2019
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=== Peak ===
=== Peak ===
360 frames (0.5° oscillation) at the peak wavelength were collected after the high-remote data. They can be downloaded from [ftp://turn5.biologie.uni-konstanz.de/pub/xds-datared/3csl/ here] (1.9 Gb). This peak dataset is somewhat difficult to index; if the results are really bad (e.g. distance refining far away from 370 mm) with the default 180 frames, then just try with 90 or 270 frames.
360 frames (0.5° oscillation) at the peak wavelength were collected after the high-remote data. They can be downloaded from [ftp://{{SERVERNAME}}/pub/xds-datared/3csl/ here] (1.9 Gb). This peak dataset is somewhat difficult to index; if the results are really bad (e.g. distance refining far away from 370 mm) with the default 180 frames, then just try with 90 or 270 frames.


This is an excerpt from [[CORRECT.LP]] :
This is an excerpt from [[CORRECT.LP]] :
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=== High-remote ===
=== High-remote ===


Due to a beamline problem, high-remote data collection stopped after 269 frames of 0.5° (the final frame is already affected). After restart of the beamline, another 100 frames were collected but they later turned out to merge badly with the first 269 frames - a hint that the monochromator was still heating up, or similar. So the latter frames were left out. The 269 frames are [ftp://turn5.biologie.uni-konstanz.de/pub/xds-datared/3csl/ here] (1.4 Gb; you guessed that the file is called 3csl-hrem.tar, right?).
Due to a beamline problem, high-remote data collection stopped after 269 frames of 0.5° (the final frame is already affected). After restart of the beamline, another 100 frames were collected but they later turned out to merge badly with the first 269 frames - a hint that the monochromator was still heating up, or similar. So the latter frames were left out. The 269 frames are [ftp://{{SERVERNAME}}/pub/xds-datared/3csl/ here] (1.4 Gb; you guessed that the file is called 3csl-hrem.tar, right?).


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From CORRECT.LP :
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=== Inflection ===
=== Inflection ===


360 frames (0.5° oscillation) at the inflection wavelength were collected after the peak data. They can be downloaded from [ftp://turn5.biologie.uni-konstanz.de/pub/xds-datared/3csl/ here] (1.8 Gb).
360 frames (0.5° oscillation) at the inflection wavelength were collected after the peak data. They can be downloaded from [ftp://{{SERVERNAME}}/pub/xds-datared/3csl/ here] (1.8 Gb).


CORRECT.LP has:
CORRECT.LP has:
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== Availability of data ==
== Availability of data ==


There are files with amplitudes (3csl-pk-F.mtz, 3csl-rh-F.mtz, 3csl-ip-F.mtz) and intensities (3csl-pk-I.mtz, 3csl-rh-I.mtz, 3csl-ip-I.mtz) as well as mad_i.pdb and mad_i.phs (written by SHELXE) available from [ftp://turn5.biologie.uni-konstanz.de/pub/xds-datared/3csl/]. Furthermore the raw data can be downloaded there.
There are files with amplitudes (3csl-pk-F.mtz, 3csl-rh-F.mtz, 3csl-ip-F.mtz) and intensities (3csl-pk-I.mtz, 3csl-rh-I.mtz, 3csl-ip-I.mtz) as well as mad_i.pdb and mad_i.phs (written by SHELXE) available from [ftp://{{SERVERNAME}}/pub/xds-datared/3csl/]. Furthermore the raw data can be downloaded there.


=== additional information for those who want to complete the structure ===
=== additional information for those who want to complete the structure ===